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. 2014 Aug 1;70(Pt 9):o935. doi: 10.1107/S160053681401678X
Stoe IPDS 2 diffractometer 3219 independent reflections
Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus 2071 reflections with I > 2σ(I)
Plane graphite monochromator Rint = 0.229
Detector resolution: 6.67 pixels mm-1 θmax = 28.4°, θmin = 3.3°
ω scans h = −12→12
Absorption correction: integration (X-RED32; Stoe & Cie, 2002) k = −8→7
Tmin = 0.962, Tmax = 0.983 l = −17→17
8493 measured reflections