| Stoe IPDS 2 diffractometer | 3219 independent reflections |
| Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus | 2071 reflections with I > 2σ(I) |
| Plane graphite monochromator | Rint = 0.229 |
| Detector resolution: 6.67 pixels mm-1 | θmax = 28.4°, θmin = 3.3° |
| ω scans | h = −12→12 |
| Absorption correction: integration (X-RED32; Stoe & Cie, 2002) | k = −8→7 |
| Tmin = 0.962, Tmax = 0.983 | l = −17→17 |
| 8493 measured reflections |