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. 2014 Aug 1;70(Pt 9):o928–o929. doi: 10.1107/S1600536814016511
Bruker X8 Proteum diffractometer 2010 independent reflections
Radiation source: Bruker MicroStar microfocus rotating anode 1904 reflections with I > 2σ(I)
Helios multilayer optics monochromator Rint = 0.042
Detector resolution: 10.7 pixels mm-1 θmax = 64.6°, θmin = 4.4°
φ and ω scans h = −2→6
Absorption correction: multi-scan (SADABS; Bruker, 2013) k = −12→12
Tmin = 0.604, Tmax = 0.662 l = −23→22
6298 measured reflections