| Bruker X8 Proteum diffractometer | 2010 independent reflections |
| Radiation source: Bruker MicroStar microfocus rotating anode | 1904 reflections with I > 2σ(I) |
| Helios multilayer optics monochromator | Rint = 0.042 |
| Detector resolution: 10.7 pixels mm-1 | θmax = 64.6°, θmin = 4.4° |
| φ and ω scans | h = −2→6 |
| Absorption correction: multi-scan (SADABS; Bruker, 2013) | k = −12→12 |
| Tmin = 0.604, Tmax = 0.662 | l = −23→22 |
| 6298 measured reflections |