Bruker Kappa APEXII diffractometer | 4305 independent reflections |
Radiation source: fine-focus sealed tube | 2837 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.041 |
Detector resolution: 0 pixels mm-1 | θmax = 27.0°, θmin = 1.9° |
ω and φ scans | h = −12→13 |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | k = −27→27 |
Tmin = 0.958, Tmax = 0.986 | l = −11→11 |
17079 measured reflections |