Skip to main content
. 2014 Sep 30;70(Pt 10):2544–2557. doi: 10.1107/S1399004714013376

Notes are the same as for Table 1 except that anomalous CC, RACC and ΔF/σ(ΔF) were evaluated from data truncated to d min = 3.5 Å.

Crystal/data set YetJ-1 YetJ-2 YetJ-3 YetJ-4 YetJ-5 YetJ-6 YetJ-7
Unit-cell parameters
a (Å) 62.90 61.98 61.91 62.07 62.09 62.08 61.60
b (Å) 288.07 287.41 287.76 287.38 287.74 286.60 288.71
No. of frames 720 × 2 720 × 2 600 × 2 360 × 2 360 × 2 360 × 2 360 × 2
Rotation span (°) 360 × 2 360 × 2 300 × 2 180 × 2 360 × 2 360 × 2 360 × 2
Bragg spacings (Å) 40–3.19 (3.27–3.19) 40–3.18 (3.27–3.18) 40–3.21 (3.29–3.21) 40–3.19 (3.28–3.19) 40–3.20 (3.28–3.20) 40–3.20 (3.29–3.20) 40–2.80 (2.87–2.80)
Total reflections 465641 462985 384208 233004 457338 457168 530451
Unique reflections 6158 6174 6051 6138 6118 6077 8507
Multiplicity 75.6 (63.5) 75.0 (56.8) 63.5 (59.5) 38.0 (32.7) 74.8 (68.0) 75.2 (69.7) 62.4 (23.8)
Completeness (%) 99.7 (96.3) 99.7 (96.3) 99.8 (98.2) 99.8 (98.6) 99.8 (98.2) 99.9 (99.1) 96.9 (83.3)
R meas 0.201 (1.397) 0.385 (2.582) 0.236 (1.773) 0.347 (2.108) 0.279 (1.604) 0.281 (1.753) 0.129 (0.870)
R p.i.m. 0.030 (0.229) 0.057 (0.432) 0.039 (0.304) 0.073 (0.482) 0.042 (0.257) 0.042 (0.277) 0.021 (0.236)
I/σ(I)〉 35.6 (4.3) 20.7 (2.2) 29.9 (3.2) 15.5 (2.0) 23.6 (3.7) 26.4 (3.6) 39.9 (4.3)
〈ΔF/σ(ΔF)〉 1.03 0.88 0.93 0.84 0.92 0.96 1.39
RACC (%) [rank] 34.2 [5′] 25.5 [10′] 33.2 [6′] 21.2 [11′] 28.5 [9′] 29.6 [8′] 32.5 [7′]
Anomalous CC (%) 26.3 8.3 12.5 3.6 22.5 21.1 54.4