Notes are the same as for Table 1 ▶ except that anomalous CC, RACC and ΔF/σ(ΔF) were evaluated from data truncated to d min = 3.5 Å.
| Crystal/data set | YetJ-1 | YetJ-2 | YetJ-3 | YetJ-4 | YetJ-5 | YetJ-6 | YetJ-7 |
|---|---|---|---|---|---|---|---|
| Unit-cell parameters | |||||||
| a (Å) | 62.90 | 61.98 | 61.91 | 62.07 | 62.09 | 62.08 | 61.60 |
| b (Å) | 288.07 | 287.41 | 287.76 | 287.38 | 287.74 | 286.60 | 288.71 |
| No. of frames | 720 × 2 | 720 × 2 | 600 × 2 | 360 × 2 | 360 × 2 | 360 × 2 | 360 × 2 |
| Rotation span (°) | 360 × 2 | 360 × 2 | 300 × 2 | 180 × 2 | 360 × 2 | 360 × 2 | 360 × 2 |
| Bragg spacings (Å) | 40–3.19 (3.27–3.19) | 40–3.18 (3.27–3.18) | 40–3.21 (3.29–3.21) | 40–3.19 (3.28–3.19) | 40–3.20 (3.28–3.20) | 40–3.20 (3.29–3.20) | 40–2.80 (2.87–2.80) |
| Total reflections | 465641 | 462985 | 384208 | 233004 | 457338 | 457168 | 530451 |
| Unique reflections | 6158 | 6174 | 6051 | 6138 | 6118 | 6077 | 8507 |
| Multiplicity | 75.6 (63.5) | 75.0 (56.8) | 63.5 (59.5) | 38.0 (32.7) | 74.8 (68.0) | 75.2 (69.7) | 62.4 (23.8) |
| Completeness (%) | 99.7 (96.3) | 99.7 (96.3) | 99.8 (98.2) | 99.8 (98.6) | 99.8 (98.2) | 99.9 (99.1) | 96.9 (83.3) |
| R meas | 0.201 (1.397) | 0.385 (2.582) | 0.236 (1.773) | 0.347 (2.108) | 0.279 (1.604) | 0.281 (1.753) | 0.129 (0.870) |
| R p.i.m. | 0.030 (0.229) | 0.057 (0.432) | 0.039 (0.304) | 0.073 (0.482) | 0.042 (0.257) | 0.042 (0.277) | 0.021 (0.236) |
| 〈I/σ(I)〉 | 35.6 (4.3) | 20.7 (2.2) | 29.9 (3.2) | 15.5 (2.0) | 23.6 (3.7) | 26.4 (3.6) | 39.9 (4.3) |
| 〈ΔF/σ(ΔF)〉 | 1.03 | 0.88 | 0.93 | 0.84 | 0.92 | 0.96 | 1.39 |
| RACC (%) [rank] | 34.2 [5′] | 25.5 [10′] | 33.2 [6′] | 21.2 [11′] | 28.5 [9′] | 29.6 [8′] | 32.5 [7′] |
| Anomalous CC (%) | 26.3 | 8.3 | 12.5 | 3.6 | 22.5 | 21.1 | 54.4 |