Table 2. Data-collection and reduction statistics for EGFRK at 6 keV.
Notes are the same as for Table 1 ▶ except that anomalous CC, RACC and ΔF/σ(ΔF) were evaluated from data truncated to d min = 4.0 Å. In this table and Tables 3 and 4, the use of the inverse-beam mode of data collection is denoted by N × 2, where N is the number of frames.
| Crystal/data | EGFRK-1 | EGFRK-2 | EGFRK-3 | EGFRK-4 | Merged 1 to 4 | Merged (3) |
|---|---|---|---|---|---|---|
| Unit-cell parameter a (Å) | 146.17 | 146.60 | 146.86 | 145.72 | 146.34 | 146.16 |
| No. of frames | 720 × 2 | 720 × 2 | 720 × 2 | 720 × 2 | 5760 | 4320 |
| Rotation span (°) | 360 × 2 | 360 × 2 | 360 × 2 | 360 × 2 | 2880 | 2160 |
| Bragg spacings (Å) | 40–3.20 (3.29–3.20) | 40–3.20 (3.29–3.20) | 40–3.20 (3.29–3.20) | 40–3.20 (3.29–3.20) | 40–3.20 (3.29–3.20) | 40–3.20 (3.29–3.20) |
| Total reflections | 742205 | 752241 | 751501 | 728119 | 2966150 | 2218779 |
| Unique reflections | 8743 | 8810 | 8867 | 8666 | 8749 | 8731 |
| Multiplicity | 84.9 (69.9) | 85.4 (75.8) | 84.8 (71.7) | 84.0 (67.4) | 339.0 (285.4) | 254.1 (211.0) |
| Completeness (%) | 100.0 (100.0) | 100.0 (100.0) | 100.0 (100.0) | 100.0 (100.0) | 100.0 (100.0) | 100.0 (100.0) |
| R meas | 0.122 (1.519) | 0.199 (3.123) | 0.236 (4.250) | 0.118 (1.660) | 0.319 (2.623) | 0.229 (2.013) |
| R p.i.m. | 0.018 (0.250) | 0.030 (0.498) | 0.035 (0.697) | 0.018 (0.277) | 0.024 (0.217) | 0.020 (0.192) |
| 〈I/σ(I)〉 | 50.0 (4.6) | 35.4 (2.7) | 27.3 (1.8) | 49.9 (4.0) | 48.5 (5.6) | 50.3 (6.1) |
| 〈ΔF/σ(ΔF)〉 | 1.52 (0.86) | 1.24 (0.78) | 1.10 (0.75) | 1.69 (0.93) | 1.34 (0.73) | 1.39 (0.79) |
| RACC (%) [rank] | 84.0 [1′] | 80.1 [2′] | 52.1 [4′] | 73.2 [3′] | 100.0 | — |
| Anomalous CC (%) | 73.6 | 60.3 | 56.2 | 78.3 | 51.1 | 70.7 |