Table 2. Structure refinement.
Values in parentheses are for the outer shell.
| Resolution range () | 35.6301.799 (1.8461.799) |
| No. of reflections | 40082 (2851) |
| Final R cryst | 0.178 (0.221) |
| Final R free | 0.221 (0.273) |
| Total unique observations | 40082 |
| No. of non-H atoms | |
| Protein | 2916 |
| Solvent (sulfate and glycerol) | 26 |
| FMN | 31 |
| Water | 239 |
| R.m.s. deviations | |
| Bonds () | 0.026 |
| Angles () | 2.02 |
| Overall mean B factor (2) | 21.6 |