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. 2014 Sep 25;70(Pt 10):1328–1332. doi: 10.1107/S2053230X14018962

Table 2. Structure refinement.

Values in parentheses are for the outer shell.

Resolution range () 35.6301.799 (1.8461.799)
No. of reflections 40082 (2851)
Final R cryst 0.178 (0.221)
Final R free 0.221 (0.273)
Total unique observations 40082
No. of non-H atoms
Protein 2916
Solvent (sulfate and glycerol) 26
FMN 31
Water 239
R.m.s. deviations
Bonds () 0.026
Angles () 2.02
Overall mean B factor (2) 21.6