Table 3. Experimentally Fit XAS Pre-Edge Positions and Areasa.
compd | peak 1 (eV); area | peak 2 (eV); area |
---|---|---|
(iPrCNC)FeBr2 | 7112.0; 11.9(9) | NA |
(iPrPDI)FeCl2b | 7111.8; 8(3) | 7113.5(3); 8(4) |
(iPrCNC)Fe(N2)2 | 7112.4; 13(1) | 7113.8; 8.1(7) |
(iPrPDI)Fe(N2)2b | 7111.9; 6.4(1) | 7114.0; 19.8(4) |
(iPrCNC)Fe(DMAP)(N2) | 7112.0; 2.4(5) | 7113.3; 14(1) |
(iPrPDI)Fe(DMAP)b | 7111.1; 13.3(3) | 7115.0; 20.2(1) |
(iPrCNC)Fe(CO)2 | 7112.8; 13.5(1) | 7114.5; 8.0(1) |
(iPrPDI)Fe(CO)2b | 7112.4; 10.2(1) | 7114.5; 16.6(2) |