Table 4. Impact of KF Stoichiometry on Yield and Selectivity.
KF (equiv) | yield (PhF) | yield (MesF) | PhF:MesF |
---|---|---|---|
0.5 | 37% | <1% | >99:1 |
1.0 | 83% | 1% | 99:1 |
1.2 | 74% | 2% | 98:2 |
1.5 | 25% | 22% | 53:47 |
2.0 | 10% | 40% | 20:80 |
3.0 | 9% | 34% | 21:79 |
KF (equiv) | yield (PhF) | yield (MesF) | PhF:MesF |
---|---|---|---|
0.5 | 37% | <1% | >99:1 |
1.0 | 83% | 1% | 99:1 |
1.2 | 74% | 2% | 98:2 |
1.5 | 25% | 22% | 53:47 |
2.0 | 10% | 40% | 20:80 |
3.0 | 9% | 34% | 21:79 |