Table 1.
Carbon | 13C data(DMSO) | |||
1 50MHz |
Lit1* | Comp 2 50MHz |
Lit2* | |
2 | 163.3 | 163.9 | 156.6 | 156.3 |
3 | 103.1 | 102.4 | 133.8 | 133.1 |
4 | 182.8 | 181.0 | 177.9 | 177.0 |
5 | 161.8 | 161.0 | 161.7 | 161.4 |
6 | 98.8 | 98.1 | 99.1 | 99.7 |
7 | 164.6 | 162.5 | 164.6 | 164.5 |
8 | 104.7 | 104.6 | 93.9 | 94.51 |
9 | 156.7 | 155.9 | 156.8 | 156.2 |
10 | 105.3 | 104.0 | 104.4 | 103.8 |
1′ | 122.3 | 121.5 | 121.6 | 121.2 |
2′ | 129.6 | 128.8 | 115.7 | 115.2 |
3′ | 116.5 | 115.7 | 145.3 | 145.1 |
4′ | 161.1 | 160.3 | 148.9 | 149.0 |
5′ | 116.5 | 115.7 | 115.7 | 115.9 |
6′ | 129.6 | 128.8 | 122.0 | 122.8 |
1′ | 74.1 | 73.3 | 101.3 | 101.6 |
2′ | 71.5 | 70.8 | 74.5 | 73.5 |
3′ | 79.3 | 78.8 | 78.0 | 77.0 |
4′ | 71.2 | 70.5 | 70.3 | 68.8 |
5′ | 82.5 | 81.7 | 76.9 | 76.6 |
6′ | 62.0 | 61.3 | 61.4 | 63.4 |
1″ | 121.6 | 121.0 | ||
2‴/6‴ | 132.0 | 133.1 | ||
3‴/5‴ | 116.6 | 116.6 | ||
4‴ | 161.7 | 163.5 | ||
7‴ | 167.4 | 167.6 |