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. Author manuscript; available in PMC: 2014 Oct 27.

Published in final edited form as: J Am Chem Soc. 2013 Mar 11;135(11):4333–4363. doi: 10.1021/ja3109664

Scheme 18 — Organometallic reactions on peptides in aqueous solution. Bottom: HPLC chromatograms of reactions. For each, top panel: starting material used for that reaction, bottom panel: crude HPLC of reaction products. ^a

^a R^N′ = Ac-Thr(OtBu)-Tyr(OtBu)-, R^C′ = -Asn(Trt)-NHRink-Resin. R^N = Ac-Thr-Tyr-, R^C = - Asn-NH₂.

Scheme 18 — Organometallic reactions on peptides in aqueous solution. Bottom: HPLC chromatograms of reactions. For each, top panel: starting material used for that reaction, bottom panel: crude HPLC of reaction products. ^a

^a R^N′ = Ac-Thr(OtBu)-Tyr(OtBu)-, R^C′ = -Asn(Trt)-NHRink-Resin. R^N = Ac-Thr-Tyr-, R^C = - Asn-NH₂.