Table 2. Yield of H2 from the Reaction of [1]0 (4.2 mM in CH2Cl2) with Various Amounts of [H(OEt2)2]BArF4a.
amt of H+, equiv | amt of H2, equiv |
---|---|
2.0 | 0.30 ± 0.09 |
5.0 | 0.45 ± 0.08 |
10.0 | 0.56 ± 0.09 |
20.0 | 0.47 ± 0.07 |
GC analyses were performed 30 min after addition of components. Yields were obtained in triplicate unless otherwise noted (see the Experimental Section).