. 2014 Jul 1;33(20):5897–5906. doi: 10.1021/om5004013

Table 3. Yield of H₂ by Treatment of [1]⁰ (4.2 mM in CH₂Cl₂) with [H(OEt₂)₂]BAr^F₄ and Fc* at −15 °C^a.

amt of 1, equiv	amt of H⁺, equiv	amt of Fc*, equiv	solvent	amt of H₂, equiv
1	5	0	CH₂Cl₂	0.45 ± 0.08
1	5	1	CH₂Cl₂	1.1 ± 0.2
1	5	4	CH₂Cl₂	1.5 ± 0.3
1	5	10	CH₂Cl₂	1.5 ± 0.3
1	10	5	CH₂Cl₂	3.3 ± 0.3
1	10	5	MeCN	0.28 ± 0.03
0	10	5	CH₂Cl₂	0.01 ± 0.01

GC analysis was performed 30 min after addition of components.

Table 3. Yield of H2 by Treatment of [1]0 (4.2 mM in CH2Cl2) with [H(OEt2)2]BArF4 and Fc* at −15 °Ca.