Table 1. Nomenclature and Site-Specific Labeling of the httNTQ30P10K2 Peptidesa.
labeling | sequenceb | |
---|---|---|
LQP-labeled | U-13C,15N-[L7, Q47, P48] | MATLEKLMKAFESLKSF-QQQ26QQPP9K2 |
LAQ-labeled | U-13C,15N-[L4, A10, Q46] | MATLEKLMKAFESLKSF-QQQ26QQPP9K2 |
MA-labeled | U-13C,15N-[M8, A10] | MATLEKLMKAFESLKSF-QQQ26QQPP9K2 |
LKSQ-labeled | U-13C,15N-[L4, K6, S16, Q19] | MATLEKLMKAFESLKSF-QQQ26QQPP9K2 |
MF-labeled | U-13C,15N-[M8, F11] | MATLEKLMKAFESLKSF-QQQ26QQPP9K2 |
MAS ssNMR samples contained approximately 8 mg of peptide (with the exception of 1.8 mg in the LKSQ-labeled peptide sample27).
Isotopically labeled residues are underlined.