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. 2014 Oct 28;9(10):e110924. doi: 10.1371/journal.pone.0110924

Table 3. Sequences for Cys32-Cys250 peptide fragments at 3451.17 (m/z) analyzed by MALDI-TOF-MS/MS.

Sequence calculated observed ppm
SAD 247.25 247.24 −40.45
IGDCR 557.63 557.61 −35.87
ELERVIGDC 989.16 989.28 121.30
LERVIGDCR 1028.23 1028.16 −68.08
SADLOTNGCVTTA 1264.41 1264.56 118.62
VTTARPVPKHIR 1401.69 1401.73 28.54
ERVIGDCR–GCVTTARPVPKHIR 2461.96 2461.98 8.12
LERVIGDCR–CVTTARPVPKHIR 2503.06 2503.38 127.83
DCR–ADLQTNGCVTTARPVPKHIR 2521.98 2522.33 138.76
ELERVIGDCR–DLQTNGCVTTARPVPKHIR 3294.82 3294.85 9.11

Values of observed M+H+ (Da) are the results of MALDI-TOF-MS/MS in Figure 1c. Mass for each fragments were calculated according to the standard fragmentation pattern.