Fig. 2.
In vitro S-glutathionylated BSA (BSA-SSG) and validation of the method using controls. 1 Electropherograms of Dylight 488 maleimide; 2 BSA-SSG; 3 BSA-SSG without Grx reduction; 4 BSA-SSG pretreated with DTT; 5 native BSA. Hydrodynamic injection at pH 8 and 11 kPa for 4 s; separation in gel containing 15% dextran (64–76 kDa), 0.5% SDS, 20 mM Tris, and 20 mM Tricine at −570 V/cm. 1, 2 Indicate Dylight 488 maleimide. Top trace is offset in the Y axis for the clarity