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. 2014 Jun 3;136(24):8568–8576. doi: 10.1021/ja504886x

Table 2. Arylation with Aryl Triflatesa.

2.2.

2.2.

a

Conditions: ArOTf (2–4 equiv), Ar–H (1 equiv), TMPLi (4–6 equiv), Et2O/THF solvent (30–40/1), −78 °C, 18 h, 0.25 mmol scale. Yields are isolated yields. See Supporting Information for details.

b

Base: LDA, THF solvent.

c

Time: 12 h in THF at −85 °C.