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. 2014 Nov;15(11):929–939. doi: 10.1631/jzus.B1400035

Table 6.

Stability of the analytes in rat plasma

Analyte Conc. added (ng/ml) Short-term stability
Autosampler stability
Freeze-thaw stability (three cycles)
Four-week stability
Conc. found (%) RSD (%) Conc. found (%) RSD (%) Conc. found (%) RSD (%) Conc. found (%) RSD (%)
GC 2.5 98.42±5.67 5.76 95.28±9.00 9.45 97.15±10.03 10.32 98.10±7.21 7.35
10 101.02±4.35 4.31 104.95±2.84 2.71 102.94±3.48 3.38 103.76±8.29 7.99
50 103.40±9.78 9.46 97.40±5.16 5.29 98.37±4.81 4.89 97.57±3.42 3.51
BB 12.5 87.60±4.52 5.16 84.59±10.79 12.76 90.10±5.27 5.85 105.67±10.12 9.58
50 97.56±4.66 4.78 122.30±2.19 1.79 109.64±5.00 4.56 96.74±9.01 9.31
250 105.12±10.24 9.74 100.84±5.90 5.85 102.29±5.30 5.18 97.11±10.08 10.38
QCT 2.5 101.65±3.41 3.35 104.43±7.73 7.40 98.72±6.81 6.90 101.31±11.09 10.95
10 104.42±4.56 4.37 113.21±7.98 7.05 101.21±8.75 8.65 97.10±7.23 7.45
50 101.74±7.88 7.75 98.97±9.05 9.14 105.31±7.64 7.25 102.35±8.22 8.03
GB 6.25 93.72±5.67 6.05 105.71±3.57 3.37 105.20±9.27 8.81 98.70±8.34 8.45
25 98.67±6.78 6.87 114.43±1.55 1.35 104.52±5.65 5.41 100.78±5.48 5.44
125 104.14±7.99 7.67 108.76±5.10 4.69 110.19±3.39 3.07 95.77±5.63 5.88
GA 12.5 106.24±10.34 9.73 79.73±5.88 7.37 89.05±4.91 5.51 97.70±6.80 6.96
50 109.12±4.01 3.67 118.25±3.20 2.71 103.68±6.47 6.24 101.21±5.84 5.77
250 90.31±6.74 7.46 89.14±3.13 3.52 90.97±2.98 3.28 98.81±4.45 4.50
KMF 2.5 107.34±5.43 5.06 96.83±9.89 10.21 96.55±7.32 7.58 97.99±7.22 7.37
10 100.72±2.45 2.43 98.73±4.82 4.88 104.93±7.54 7.19 102.31±6.78 6.63
50 98.97±3.21 3.24 102.3±7.15 6.99 99.74±8.71 8.73 108.98±12.11 11.11
ISR 2.5 104.54±4.54 4.34 87.98±5.75 6.54 89.74±5.25 5.85 101.16±9.12 9.02
10 101.23±6.77 6.69 112.32±5.78 5.15 101.72±5.67 5.57 103.45±7.76 7.50
50 98.78±7.68 7.77 100.44±6.91 6.88 105.50±9.78 9.27 98.79±6.34 6.42

The values for the concentration found are expressed as mean±SD, n=3. GC: ginkgolide C; BB: bilobalide; QCT: quercetin; GB: ginkgolide B; GA: ginkgolide A; KMF: kaempferol; ISR: isorhamnetin; RSD: relative standard deviation