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. Author manuscript; available in PMC: 2015 Oct 6.
Published in final edited form as: Angew Chem Int Ed Engl. 2014 Sep 4;53(41):11075–11078. doi: 10.1002/anie.201406819

Table 1.

Scope exploration.[a]

entry diene aldehyde product yield[b]
(ee)
1 graphic file with name nihms-637149-t0007.jpg 1 graphic file with name nihms-637149-t0008.jpg 72%
(85%)
2 2 graphic file with name nihms-637149-t0009.jpg graphic file with name nihms-637149-t0010.jpg 50
(>99%)
3 2 graphic file with name nihms-637149-t0011.jpg graphic file with name nihms-637149-t0012.jpg 53
(84%)
4 graphic file with name nihms-637149-t0013.jpg 1 graphic file with name nihms-637149-t0014.jpg 71
(>99%)[c]
5 graphic file with name nihms-637149-t0015.jpg 1 graphic file with name nihms-637149-t0016.jpg 75
(>99%)[c]
[a]

See the Supporting Information for detailed procedures, substrate syntheses, and stereochemical determination.

[b]

Yield of isolated, purified product.

[c]

Diastereomeric products were removed by chromatography.