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. Author manuscript; available in PMC: 2015 Mar 26.
Published in final edited form as: Curr Protoc Nucleic Acid Chem. 2014 Mar 26;5(514):5.14.1–5.14.15. doi: 10.1002/0471142700.nc0514s56

Table 1.

Synthesis of N2-[3-[(trifluoroacetyl)amino]propyl]-O6-(trimethylsilylethyl)-2′-deoxyguanosine (2) starting from 1

Reagent Amount MW (g/mol) Millimoles Equivalents
N2-(3-aminopropyl)-O6-(trimethylsilylethyl)-2′-deoxyguanosine 0.2 g 324 0.58 1
Ethyl trifluoroacetate 56 μl 142 0.75 1.3
Methanol, anhydrous 6 mL 32 140 255