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. Author manuscript; available in PMC: 2015 Nov 7.
Published in final edited form as: J Chromatogr A. 2014 Sep 22;1367:154–160. doi: 10.1016/j.chroma.2014.09.040

Table 1.

Effect of temperature on the B/F ratio using 4.5 kV separation voltage.

Temperature (°C)* B/F RSD (%)**
No Cooling 28 1.43 3.50
Air Cooling 26 3.53 1.13
Active Cooling 25.0 4.49 1.33
23.0 5.31 1.50
21.0 5.76 1.38
19.0 4.80 0.62
17.0 2.39 1.25
*

The precision of the temperature at 28 °C was ± 1 °C, at 26 °C was ± 0.4 °C, and for others were ± 0.1°C

**

The standard deviations reported were determined from 5 consecutive separations