Table 2. Experimental details.
| Crystal data | |
| Chemical formula | |
| M r | 412.99 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 295 |
| a, b, c () | 7.6270(17), 7.2603(16), 13.580(3) |
| () | 91.91(2) |
| V (3) | 751.6(3) |
| Z | 2 |
| Radiation type | Ag K, = 0.56085 |
| (mm1) | 0.72 |
| Crystal size (mm) | 0.20 0.20 0.20 |
| Data collection | |
| Diffractometer | EnrafNonius CAD-4 |
| Absorption correction | scan (North et al., 1968 ▶) |
| T min, T max | 0.945, 0.958 |
| No. of measured, independent and observed [I > 2(I)] reflections | 1706, 1640, 1215 |
| R int | 0.021 |
| (sin /)max (1) | 0.638 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.035, 0.077, 1.02 |
| No. of reflections | 1640 |
| No. of parameters | 140 |
| No. of restraints | 3 |
| max, min (e 3) | 0.34, 0.31 |