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. 2014 Oct 24;70(Pt 11):o1185–o1186. doi: 10.1107/S1600536814023046
Bruker APEXII CCD diffractometer 3945 independent reflections
Radiation source: fine-focus sealed tube 2911 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.022
Detector resolution: 0 pixels mm-1 θmax = 31.0°, θmin = 2.5°
ω and φ scans h = −10→10
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) k = −12→12
Tmin = 0.897, Tmax = 0.917 l = −18→17
20157 measured reflections