| Bruker APEXII CCD diffractometer | 3945 independent reflections |
| Radiation source: fine-focus sealed tube | 2911 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.022 |
| Detector resolution: 0 pixels mm-1 | θmax = 31.0°, θmin = 2.5° |
| ω and φ scans | h = −10→10 |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | k = −12→12 |
| Tmin = 0.897, Tmax = 0.917 | l = −18→17 |
| 20157 measured reflections |