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. 2014 Oct 24;70(Pt 11):o1197–o1198. doi: 10.1107/S160053681402323X
Bruker APEXII CCD diffractometer 5269 independent reflections
Radiation source: fine-focus sealed tube 4426 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.035
Detector resolution: 7.9 pixels mm-1 θmax = 27.9°, θmin = 1.7°
ω and φ scans h = −12→11
Absorption correction: multi-scan (SADABS; Bruker, 2014) k = −14→14
Tmin = 0.865, Tmax = 0.947 l = −16→16
37843 measured reflections