| Bruker APEXII CCD diffractometer | 5269 independent reflections |
| Radiation source: fine-focus sealed tube | 4426 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.035 |
| Detector resolution: 7.9 pixels mm-1 | θmax = 27.9°, θmin = 1.7° |
| ω and φ scans | h = −12→11 |
| Absorption correction: multi-scan (SADABS; Bruker, 2014) | k = −14→14 |
| Tmin = 0.865, Tmax = 0.947 | l = −16→16 |
| 37843 measured reflections |