| Crystal data |
| Chemical formula |
[NaNi(C18H18N2O4)(NO3)(CH4O)] |
|
M
r
|
502.09 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c () |
7.207(1), 11.047(1), 13.619(1) |
| , , () |
95.30(1), 99.81(1), 99.05(1) |
|
V (3) |
1047.2(2) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
1.00 |
| Crystal size (mm) |
0.4 0.2 0.2 |
| |
| Data collection |
| Diffractometer |
Nonius KappaCCD |
| Absorption correction |
Multi-scan (SADABS; Sheldrick, 2003 ▶) |
|
T
min, T
max
|
0.690, 0.825 |
| No. of measured, independent and observed [I > 2(I)] reflections |
12718, 6501, 4324 |
|
R
int
|
0.020 |
| (sin /)max (1) |
0.744 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.035, 0.081, 0.90 |
| No. of reflections |
6501 |
| No. of parameters |
292 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.50, 0.32 |
