Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [CoSn3(CH3)9(C14H10)] |
| M r | 728.52 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 173 |
| a, b, c () | 12.9784(18), 13.0834(18), 16.734(2) |
| , , () | 72.754(2), 75.891(2), 89.551(2) |
| V (3) | 2625.5(6) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 3.45 |
| Crystal size (mm) | 0.28 0.24 0.06 |
| Data collection | |
| Diffractometer | Siemens SMART CCD platform |
| Absorption correction | Multi-scan (SADABS; Sheldrick, 2012 ▶) |
| T min, T max | 0.493, 0.746 |
| No. of measured, independent and observed [I > 2(I)] reflections | 30588, 11891, 9564 |
| R int | 0.032 |
| (sin /)max (1) | 0.650 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.038, 0.086, 1.08 |
| No. of reflections | 11891 |
| No. of parameters | 639 |
| No. of restraints | 42 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| max, min (e 3) | 1.93, 0.79 |