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. 2014 Oct 31;70(Pt 11):m385–m386. doi: 10.1107/S1600536814023423
Agilent SuperNova (Dual, Cu at zero, Atlas) diffractometer 3943 independent reflections
Radiation source: sealed X-ray tube, SuperNova (Cu) X-ray Source 2557 reflections with I > 2σ(I)
Mirror monochromator Rint = 0.059
Detector resolution: 10.6191 pixels mm-1 θmax = 66.6°, θmin = 3.4°
ω scans h = −4→7
Absorption correction: analytical [CrysAlis PRO (Agilent, 2014), based on expressions derived by Clark & Reid (1995)] k = −25→26
Tmin = 0.887, Tmax = 0.971 l = −18→19
7799 measured reflections