| Agilent SuperNova (Dual, Cu at zero, Atlas) diffractometer | 3943 independent reflections |
| Radiation source: sealed X-ray tube, SuperNova (Cu) X-ray Source | 2557 reflections with I > 2σ(I) |
| Mirror monochromator | Rint = 0.059 |
| Detector resolution: 10.6191 pixels mm-1 | θmax = 66.6°, θmin = 3.4° |
| ω scans | h = −4→7 |
| Absorption correction: analytical [CrysAlis PRO (Agilent, 2014), based on expressions derived by Clark & Reid (1995)] | k = −25→26 |
| Tmin = 0.887, Tmax = 0.971 | l = −18→19 |
| 7799 measured reflections |