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. 2014 Nov 12;70(Pt 12):480–482. doi: 10.1107/S1600536814024271

Table 2. Experimental details.

Crystal data
Chemical formula [SnCl4(H2O)2]6H2O
M r 404.62
Crystal system, space group Monoclinic, C2/c
Temperature (K) 200
a, b, c () 16.0224(15), 7.8530(8), 12.6766(12)
() 119.739(7)
V (3) 1384.9(2)
Z 4
Radiation type Mo K
(mm1) 2.63
Crystal size (mm) 0.34 0.23 0.12
 
Data collection
Diffractometer Stoe IPDS 2T
Absorption correction Integration (Coppens, 1970)
T min, T max 0.492, 0.731
No. of measured, independent and observed [I > 2(I)] reflections 13041, 1600, 1451
R int 0.030
(sin /)max (1) 0.650
 
Refinement
R[F 2 > 2(F 2)], wR(F 2), S 0.021, 0.049, 1.11
No. of reflections 1600
No. of parameters 92
No. of restraints 12
H-atom treatment All H-atom parameters refined
max, min (e 3) 1.01, 0.71

Computer programs: X-AREA and X-RED (Stoe Cie, 2009), SHELXS97 and SHELXL2012 (Sheldrick, 2008), DIAMOND (Brandenburg, 2006) and publCIF (Westrip, 2010).