Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C25H25N3O |
| M r | 383.48 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 293 |
| a, b, c () | 8.8509(2), 9.6364(3), 12.9090(4) |
| , , () | 72.779(2), 81.033(1), 76.457(1) |
| V (3) | 1017.97(5) |
| Z | 2 |
| Radiation type | Mo K |
| (mm1) | 0.08 |
| Crystal size (mm) | 0.21 0.19 0.18 |
| Data collection | |
| Diffractometer | Bruker Kappa APEXII |
| Absorption correction | Multi-scan (SADABS; Bruker, 2004 ▶) |
| T min, T max | 0.967, 0.974 |
| No. of measured, independent and observed [I > 2(I)] reflections | 22986, 3798, 3177 |
| R int | 0.023 |
| (sin /)max (1) | 0.606 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.035, 0.096, 1.05 |
| No. of reflections | 3798 |
| No. of parameters | 263 |
| No. of restraints | 1 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.14, 0.13 |