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. 2014 Nov 21;70(Pt 12):544–546. doi: 10.1107/S1600536814024982
Bruker APEXII CCD diffractometer 4868 independent reflections
Radiation source: fine-focus sealed tube 3305 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.117
ω–2θ scans θmax = 30.1°, θmin = 2.2°
Absorption correction: multi-scan (SADABS; Bruker, 2009) h = −13→13
Tmin = 0.792, Tmax = 0.881 k = −13→13
14477 measured reflections l = −26→26