Table 2. Crystallization screening and refinement conditions for X. citri PhoX in the absence and presence of phosphate.
The best crystals obtained after refinement are shown in Fig. 1 ▶.
| Sample | Protein concentration (mgml1) | Screening | Refinement | Crystals | Resolution after refinement () |
|---|---|---|---|---|---|
| PhoX + sodium phosphate | 10 | 25% PEG 3350, 200mM sodium iodide, 100mM bis-tris pH 5.5 | 20% PEG 3350, 200mM sodium iodide | Fig. 1 ▶(a) | 3.0 |
| PhoX | 8 | 20% PEG 3350, 200mM sodium iodide | 17% PEG 3350, 200mM sodium iodide | Fig. 1 ▶ (b) | 5.0 |
| PhoX | 10 | 20% PEG 3350, 200mM sodium iodide | 17% PEG 3350, 250mM sodium iodide | Fig. 1 ▶(c) | 6.0 |
| PhoX + sodium phosphate | 15 | 20% PEG 3350, 200mM sodium iodide | 17% PEG 3350, 250mM sodium iodide | Fig. 1 ▶(d) | 2.9 |
| PhoX + sodium phosphate | 15 | 17% PEG 3350, 250mM sodium iodide | 15% PEG 3350, 250mM sodium iodide | Fig. 1 ▶(e) | 3.0 |