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. 2014 Nov 14;70(Pt 12):1636–1639. doi: 10.1107/S2053230X14023243

Table 3. Data collection and processing.

Values in parentheses are for the outer shell.

Diffraction source PROXIMA 1, SOLEIL
Wavelength () 0.97857
Temperature (C) 173
Detector PILATUS 6M
No. of crystals used 1
Crystal-to-detector distance (mm) 577.75
Rotation range per image () 0.2
Total rotation range () 120
Exposure time per image (s) 0.2
Space group P43212
a, b, c () 103.94, 103.94, 344.57
, , () 90, 90, 90
No. of chains per asymmetric unit 2
Solvent content (%) 62
Mosaicity () 0.09
Resolution range () 47.353.25
Total No. of reflections 216820
No. of unique reflections 30865
Completeness (%) 99.9 (100.0)
Multiplicity 7.0 (7.5)
I/(I) 19.6 (2.4)
R meas 0.116 (1.488)
Overall B factor from Wilson plot (2) 94

The correct hand was determined during the molecular-replacement search as mentioned in 3.