Table 3. Data collection and processing.

Values in parentheses are for the outer shell.

Diffraction source	BL44XU, SPring-8
Wavelength ()	0.9
Temperature (K)	100
Detector	Rayonix MX225-HE
Crystal-to-detector distance (mm)	300
Rotation range per image ()	0.8
Total rotation range ()	380
Exposure time per image (s)	1.0
Space group	P212121
a, b, c ()	90.9, 123.4, 135.4
, , ()	90, 90, 90
Mosaicity ()	0.3
Resolution range ()	50.02.6 (2.642.60)
Total No. of reflections	159905
No. of unique reflections	41285
Completeness (%)	86.8 (78.2)
Multiplicity	3.9 (2.4)
I/(I)	5.3 (2.6)
R p.i.m. † (%)	6.8 (20.5)

^† R _p.i.m. = , where N(hkl) is the mean redundancy.