Table 1. EXAFS parameters for Dy and Lu species adsorbed on salmon milt and reference materials (CN, coordination number; R, interatomic distance; ΔE0, threshold E0 shift; σ, Debye-Waller factor; least squares precisions are given to each value).
Sample | k range (Å−1) | Shell | CNa | R (Å)a | ΔE0 (eV) | σ2 (x103 Å2)a , b | Residual (%) |
Dy on CP | 2.85–8.85 | Dy-O | 10.2±1.1 | 2.329±0.020 | 4.8±2.1 | 12.1±0.2 | 1.6 |
Dy-P | 1.1±0.1 | 3.759±0.111 | 12.1±0.9 | ||||
Dy on CMC | 2.95–10.75 | Dy-O | 10.9±1.0 | 2.383±0.020 | 3.2±2.5 | 12.1±0.2 | 0.9 |
Dy-C | 2.7±0.1 | 3.401±0.19 | 5.3±0.9 | ||||
Dy on Ln resin | 2.80–10.35 | Dy-O | 9.6±2.1 | 2.249±0.016 | 3.9±2.0 | 7.6±0.8 | 1.4 |
Dy-P | 7.2±0.1 | 3.762±0.104 | 13.7* | ||||
Dy on DNA-filter hybrid, pH 3 | 2.66–9.38 | Dy-O | 11.9±2.8 | 2.343±0.020 | 2.7±2.1 | 12.1 | 0.8 |
Dy-P | 1.2±0.2 | 3.742±0.027 | 12.1* | ||||
Dy on salmon milt, pH 3 | 2.75–9.45 | Dy-O | 10.5±1.1 | 2.308±0.019 | 2.2±2.0 | 11.0 | 1.0 |
Dy-P | 2.1±0.1 | 3.795±0.027 | 6.7±0.9 | ||||
Lu on CP | 2.75–10.2 | Lu-O | 9.8±2.3 | 2.284±0.019 | 6.8±2.1 | 12.1±0.8 | 3.3 |
Lu-P | 2.3±0.1 | 3.812±0.050 | 12.1* | ||||
Lu on CMC | 2.80–10.35 | Lu-O | 10.1±2.3 | 2.298±0.019 | 6.3±2.1 | 10.8±0.8 | 1.3 |
Lu-C | 3.6±0.1 | 3.328±0.050 | 4.9* | ||||
Lu on Ln resin | 2.80–10.35 | Lu-O | 8.4±1.7 | 2.184±0.014 | 6.4±2.1 | 5.8±0.8 | 1.4 |
Lu-P | 5.3±0.3 | 3.734±0.025 | 9.6±0.8 | ||||
Lu on DNA-filter hybrid, pH 3 | 2.80–10.05 | Lu-O | 10.5±2.1 | 2.270±0.017 | 6.0±2.0 | 12.3±0.6 | 1.1 |
Lu-P | 1.9±0.1 | 3.786±0.195 | 10.0±0.6 | ||||
Lu on salmon milt, pH 3 | 2.90–10.40 | Lu-O | 8.2±1.7 | 2.203±0.015 | 6.7±2.1 | 6.7±0.8 | 1.1 |
Lu-P | 3.5±0.1 | 3.773±0.112 | 4.1 |