TABLE 1.
Data collection and refinement statistics
| pAPN-CNGRCG complex | |
|---|---|
| Data Collection | |
| Space group | C2 |
| Cell dimensions | |
| a, b, c (Å) | 260.3, 62.9, 82.0 |
| α, β, γ (°) | 90, 100.6, 90 |
| Resolution (Å) | 50-1.92 (1.96-1.92)a |
| Rsym or Rmerge | 0.079 (0.615) |
| I/σI | 20.7 (1.7) |
| Completeness (%) | 97.9 (97.0) |
| Redundancy | 3.8 (3.9) |
| Refinement | |
| Resolution (Å) | 47.73-1.95 |
| No. of reflections | 88,780 |
| Rwork/Rfree | 0.140/0.189 |
| No. of atoms | 8498 |
| Protein | 7259 |
| CNGRCG | 40 |
| B-factors (Å2) | 48.9 |
| Protein | 47.3 |
| CNGRCG | 44.0 |
| R.M.S.b derivations | |
| Bond lengths (Å) | 0.012 |
| Bond angles (°) | 1.614 |
| Ramachandran plot | |
| Favored (%) | 97 |
| Allowed (%) | 2.6 |
| Disallowed (%) | 0.4 |
a Values in parentheses are for highest resolution shell.
b R.M.S. is root mean square.