Table 4.
Sample | Equilibrium moisture uptake [wt%] |
Contact angle [°] |
Equilib- rium Tga) [°C] |
Estimated working- time b) [min] |
---|---|---|---|---|
100TM | 2.3 ± 1.0 | 78.08 ± 2.58 | 39.1 ± 0.3 | 10 |
80TM | 4.3 ± 0.7 | 74.73 ± 2.51 | 30.6 ± 1.3 | 5 |
60TM | 4.4 ± 0.9 | 74.06 ± 0.83 | 26.4 ± 0.4 | 4 |
40TM | 6.0 ± 0.8 | 70.62 ± 3.51 | 21.1 ± 1.7 | 3 |
20TM | 5.0 ± 0.8 | 66.26 ± 4.97 | 15.0 ± 0.7 | < 3 |
0TM | 8.1 ± 1.9 | 62.55 ± 2.86 | 12.2 ± 0.6 | < 1 |
Measured after 2 h of submersion in water;
Defined here as the time until ≈ 20% of the initial diameter is recovered in 37 ° C water (representative of, but not necessarily equivalent to, the working time for an actual catheter-delivered device).