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. 2014 Dec 3;5:5574. doi: 10.1038/ncomms6574

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(a) Solution-phase synchrotron small-angle X-ray-scattering profile of the solution of Com-Tetra ([PP]=8 mM) in water. (b) Solution-phase synchrotron X-ray diffraction (XRD) profile in water. (c) XRD profile of the solid sample obtained by evaporating the solution of Com-Tetra in water. The peak value was attributed by choosing the position that is highest above the straight line defined by the two saddle points of the broad peak. (d) Small-angle synchrotron X-ray-scattering profile of Com-Tetra of the solid sample. (e) Two-dimensional synchrotron X-ray-scattering profile of Com-Tetra of the solid sample.