Table 1. Summary of data collection statistics for PDT crystallized with 8,9-dihydro-9-oxoimidazo[2,1-b]purinea.
Parameters | Values |
Resolution (Å) | 2.1 |
Space group | P43212 |
a, b (Å) | 79.69 |
c (Å) | 186.69 |
N/ASU | 3 |
Matthews number | 2.53 |
Solvent content (%) | 55 |
Unique reflections | 35578 |
Redundancy | 5.9 (5.3) |
Completeness | 98.7 (93.6) |
Rsym b (%) | 4.6 (26.6) |
I/σ | 23.1 (4.8) |
Values for the highest resolution shell are given in parentheses.
R sym = ΣΣi Ii−<I> |/Σ<I>, where <I> is the mean intensity of the N reflections with intensities Ii and common indices h,k,l.