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. Author manuscript; available in PMC: 2016 Jan 1.
Published in final edited form as: Bioorg Med Chem. 2014 Nov 20;23(1):126–131. doi: 10.1016/j.bmc.2014.11.021

Table 1.

NMR data of 1 measured at 600 (1H) and 150 (13C) MHz (CD3OD).

No. 1
δ C δ H
1 144.1 -
2 108.0 6.13b
3 161.7 -
4 101.1 6.08
5 159.7 -
6 108.0 6.14b
1' 34.7 3.35c
2' 131.05 5.54
3' 125.3 6.35
4' 124.7 6.38
5' 133.8 5.52
6' 28.6 2.20
7' 30.34a 1.44
8' 30.38a 1.33
9' 30.44a 1.33
10' 30.63a 1.33
11' 30.69a 1.25
12' 30.76a 1.25
13' 30.86 1.37
14' 35.9 2.22
15' 135.2 -
16' 136.5 5.97 (q, J=7.1 Hz)
17' 15.9 1.92 (d, J=7.1 Hz)
18' 172.0 -
a

may be exchangeable

b

may be exchangeable

c

overlapped with solvent peak