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. Author manuscript; available in PMC: 2015 Dec 1.
Published in final edited form as: J Biomol NMR. 2014 Nov 9;60(4):219–229. doi: 10.1007/s10858-014-9870-y

Figure 4.

Figure 4

Sequential backbone walk for residues A21–A28 of LC8 using 3D fast MAS experiments: HNCA (green), HNCO (black) and HNCOCX (purple). The solid-state NMR experiments were carried out on Bruker Ascend 850 MHz spectrometer at the magnetic field of 19.9 T. All 3D spectra were recorded at the MAS frequency of 62 kHz with apparent temperature controlled at −33±1 °C (sample temperature was 2 °C).