Table 6. Hydrogen-bond geometry.

Hydrogen-bonding geometry in the LT form at 105K (Grbitz Sagstuen, 2008 ▶), in italics, is included in the table for comparison. All contacts have been recalculated with OH distances normalized to 0.985. The symmetry operations are given in Table 5 ▶

	HA ()		D A ()		DHA ()
DHA	308K	105K	308K	105K†	308K	105K
O5H5O2	1.946	1.917	2.607 (1)	2.595	122.1	123.5
O5H5O3vii	2.600	2.528	3.377 (1)	3.282	135.8	133.1
O6H6O101x	1.872	1.847 ‡	2.783 (3)	2.812 ‡	152.6	165.8 ‡
O6H6O102x	2.304		3.204 (4)		151.5
O7H17O6	1.823	1.799	2.803 (1)	2.783	172.2	176.5
O7H27O4iv	1.940	1.868	2.894 (1)	2.850	162.6	174.4
O8H18O3xiv	1.728	1.714	2.709 (1)	2.694	172.8	173.0
O8H28O2i	1.781	1.768	2.765 (1)	2.750	175.7	175.2
O9H19O2xiii	2.282	2.410	3.106 (2)	3.118	140.5	128.4
O9H19O6xi	2.428	2.279	3.152 (1)	3.103	130.0	140.5
O9H19O3xi	2.681	2.504	3.189 (2)	3.157	112.4	123.6
O9H29O4viii	1.835	1.803	2.816 (2)	2.784	173.9	173.4
O101H110O1ii	1.786	1.770 §	2.707 (5)	2.712§	157.5	158.9 §
O102H210O9i	1.833	1.796 ¶	2.713 (6)	2.753 ¶	147.8	163.1 ¶

^†E.s.d.’s in the range (0.60.8) 10³.

^‡O6H6O10^x.

^§O10H110O1ⁱⁱ.

^¶O10H210O9ⁱ.