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. 2014 Oct 23;43(46):17463–17474. doi: 10.1039/c4dt00845f

Table 2. Crystallographic parameters of C2.

Empirical formula C41H28ClIrN6O
F.w. 848.36
Cryst syst Orthorhombic
Space group P212121
a (Å) 9.650(4)
b (Å) 15.353(6)
c (Å) 25.967(11)
V3) 3847(3)
Z 4
λ (Å) 0.71073
Crystal size (mm3) 0.22 × 0.10 × 0.05
T (K) 100
ρ calcd (g cm–3) 1.465
μ (mm–1) 3.579
θ (°) 1.54–25.00
F(000) 1672
Index ranges –7 ≤ h ≤ 11
–16 ≤ k ≤ 18
–27 ≤ l ≤ 30
Data/restraints/params 6787/1/152
GOF (F 2) 0.964
R 1, wR2 (I > 2σ(I)) 0.0658, 0.1354
R 1, wR2 (all data) 0.0986, 0.1489
W 1/[σ2(Fo2) + (0.0566P)2 + 0.0000P], where P = (Fo2 + 2Fc2)/3