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. 2014 Dec 31;48(1):229–235. doi: 10.1021/ma5019044

Scheme 3. Scope of this Methodology: Ketone (511), Secondary Alcohol (1214), TMS (15), F (16), and Azide (17) Functionalized P3HTs.

Scheme 3

The conversion determined by 19F NMR with trifluorotoluene as an internal standard in NMR solvent. EA showed 46% conversion (See Supporting Information).

The conversion is slightly overestimated due to overlapped peaks in the aryl region of the 1H NMR spectra with CdCl3.

The conversion cannot be calculated with a single value due to the overlapped peaks of α-CH2 of hexyl chain with Ar-Me.

Slightly different reaction contions are employed. Please see below and Supporting Information for detailed conditions.

The conversion was not available due to the insolubility of the product.