Skip to main content
. 2015 Jan 6;2015:519854. doi: 10.1155/2015/519854

Table 2.

Thermal properties, FT-IR ratio of peaks 1047/1022 cm−1, swelling power (g/g of dry starch), and water solubility (g/g of dry starch × 100) of native JFS and selective HMT-JFS treated at conditions of 10–35% MC and 80–120°C for 16 h.

JFS sample Temperature (°C) ΔT ΔH FT-IR ratio Swelling power at T (°C) Solubility at T (°C)
T o T p T c (J/g) RT 50 60 70 80 90 RT 50 60 70 80 90
Native 82.58 ± 0.24 84.24 ± 0.37 88.63 ± 0.12 6.05 ± 0.31 11.25 ± 0.06 0.80 ± 0.01 1.1 1.3 2.3 2.5 6.8 7.7 0.4 1.3 2.4 2.8 7.2 9.5

80°C
 10% MC 82.28 ± 0.94 84.41 ± 0.54 88.75 ± 0.07 6.47 ± 0.37 10.14 ± 0.06 0.82 ± 0.03 1.1 1.3 2.1 2.9 5.3 7.0 0.5 1.5 2.2 2.9 7.2 9.3
 20% MC 82.52 ± 0.31 85.38 ± 0.24 88.25 ± 0.21 5.73 ± 0.10 7.44 ± 0.26 0.85 ± 0.02 1.0 1.4 2.3 2.9 5.0 6.7 0.7 1.5 2.3 3.1 7.1 9.2
 25% MC 86.10 ± 0.12 88.79 ± 0.39 91.65 ± 1.06 5.55 ± 0.94 7.27 ± 0.73 0.84 ± 0.02 1.1 1.5 2.5 2.8 3.2 5.7 0.7 1.7 2.3 3.2 7.3 9.1
 30% MC 89.22 ± 0.27 91.03 ± 0.13 93.25 ± 0.21 4.03 ± 0.06 4.49 ± 0.23 0.83 ± 0.03 1.1 1.2 2.4 2.7 4.3 5.5 0.6 1.6 2.5 3.0 7.2 9.2
 35% MC 89.32 ± 0.14 91.14 ± 0.16 93.40 ± 0.71 4.08 ± 0.85 5.04 ± 0.36 0.85 ± 0.04 1.2 1.2 2.6 2.6 5.0 6.1 0.5 1.7 2.6 3.1 7.3 9.6

90°C
 10% MC 82.14 ± 1.20 85.01 ± 0.63 88.05 ± 0.92 5.91 ± 0.28 9.20 ± 0.95 0.78 ± 0.06 1.0 1.2 2.3 3.1 5.9 7.3 0.4 1.4 2.3 2.9 6.8 9.1
 20% MC 85.71 ± 0.09 88.20 ± 0.40 91.90 ± 1.41 6.19 ± 1.51 8.12 ± 1.10 0.84 ± 0.04 1.1 1.5 2.7 3.3 5.5 6.9 0.4 1.5 2.4 3.2 7.0 9.3
 25% MC 91.62 ± 0.20 93.49 ± 0.55 96.20 ± 1.13 4.58 ± 0.93 7.41 ± 1.12 0.77 ± 0.05 1.1 1.4 2.6 2.9 5.6 6.7 0.3 1.6 2.4 3.1 6.8 9.2
 30% MC 90.57 ± 0.23 92.53 ± 0.16 95.00 ± 0.57 4.43 ± 0.80 5.11 ± 0.99 0.78 ± 0.06 1.0 1.3 2.5 3.2 5.3 6.2 0.4 1.5 2.6 3.1 7.0 9.3
 35% MC 91.35 ± 0.48 93.57 ± 0.56 96.50 ± 1.56 5.15 ± 1.08 4.87 ± 1.37 0.75 ± 0.05 1.0 1.4 2.7 2.9 5.4 6.6 0.4 1.8 2.6 3.0 7.0 9.5

100°C
 10% MC 81.68 ± 0.44 84.69 ± 0.45 89.00 ± 0.85 7.32 ± 0.41 10.75 ± 0.33 0.78 ± 0.03 1.1 1.3 2.2 3.1 5.6 6.5 0.5 1.2 2.3 3.0 6.6 8.9
 20% MC 85.37 ± 0.32 88.18 ± 0.51 91.75 ± 1.20 6.38 ± 0.88 8.93 ± 1.04 0.76 ± 0.03 1.1 1.2 2.3 3.2 5.2 5.8 0.4 1.1 2.3 2.9 5.7 8.2
 25% MC 89.13 ± 0.27 92.07 ± 0.03 95.25 ± 0.21 6.12 ± 0.06 5.80 ± 0.93 0.76 ± 0.05 1.0 1.2 2.5 2.9 4.8 5.4 0.5 1.1 2.4 2.8 5.0 7.5
 30% MC 92.12 ± 0.09 94.29 ± 0.05 97.60 ± 0.00 5.48 ± 0.09 4.38 ± 0.64 0.75 ± 0.03 1.0 1.1 2.2 2.8 4.0 5.3 0.5 1.3 2.3 2.7 4.7 7.2
 35% MC 93.26 ± 0.01 95.45 ± 0.07 98.05 ± 0.04 4.79 ± 0.22 1.80 ± 0.06 0.70 ± 0.05 1.1 1.1 2.2 2.5 3.3 4.6 0.4 1.1 2.2 2.6 4.4 6.9

110°C
 10% MC 81.66 ± 0.38 84.50 ± 0.27 88.25 ± 0.21 6.59 ± 0.59 9.35 ± 1.33 0.81 ± 0.01 1.0 1.3 2.3 3.2 5.8 7.2 0.3 1.3 2.4 3.4 7.0 9.0
 20% MC 84.92 ± 0.90 87.34 ± 0.15 91.55 ± 0.21 6.63 ± 1.12 3.10 ± 1.36 0.84 ± 0.02 1.0 1.3 2.4 3.2 5.4 6.8 0.3 1.3 2.5 3.5 7.2 8.8
 25% MC 86.49 ± 1.25 90.95 ± 0.12 94.80 ± 0.85 8.31 ± 0.40 4.55 ± 0.84 0.77 ± 0.05 1.2 1.6 2.7 3.3 5.5 6.5 0.4 1.2 2.5 3.4 7.2 8.7
 30% MC 89.21 ± 0.67 91.92 ± 0.66 95.75 ± 0.92 6.54 ± 0.25 4.75 ± 1.20 0.76 ± 0.03 1.2 1.4 2.7 3.4 4.9 6.1 0.4 1.3 2.6 3.7 7.3 8.9
 35% MC 89.29 ± 0.17 92.31 ± 0.18 95.55 ± 0.21 6.26 ± 0.05 1.63 ± 0.07 0.78 ± 0.04 1.2 1.5 2.8 3.6 4.8 6.5 0.4 1.4 2.5 3.6 7.6 9.4

120°C
 10% MC 81.75 ± 0.72 84.76 ± 0.73 89.05 ± 2.19 7.30 ± 1.47 9.29 ± 0.93 0.82 ± 0.02 1.1 1.2 2.2 3.2 5.7 7.0 0.5 1.6 2.2 3.3 7.4 9.2
 20% MC 86.05 ± 4.47 86.48 ± 0.21 90.65 ± 0.07 6.60 ± 0.54 4.14 ± 0.25 0.82 ± 0.03 1.1 1.3 2.4 3.3 5.9 6.8 0.4 1.6 2.3 3.4 7.3 9.3
 25% MC 87.33 ± 2.10 90.91 ± 0.14 93.90 ± 0.57 6.57 ± 0.66 3.88 ± 0.90 0.77 ± 0.05 1.3 1.4 2.5 2.9 5.5 6.6 0.5 1.8 2.3 3.6 7.5 9.6
 30% MC 86.92 ± 0.27 90.88 ± 0.96 95.80 ± 0.99 8.88 ± 1.26 3.18 ± 0.74 0.74 ± 0.04 1.3 1.5 2.6 3.1 5.5 6.9 0.5 1.9 2.5 3.5 7.4 9.4
 35% MC 88.27 ± 0.16 91.68 ± 0.19 94.75 ± 0.35 6.48 ± 0.19 2.28 ± 0.35 0.69 ± 0.03 1.2 1.5 2.6 3.4 5.8 7.2 0.5 1.6 2.6 3.3 7.5 9.5