Table 3. Data collection and processing.
Values in parentheses are for the outer shell.
| Diffraction source | ‘Belok’, NRC ‘Kurchatov Institute’ |
| Wavelength () | 0.984 |
| Temperature (K) | 100 |
| Detector | MAR CCD |
| Crystal-to-detector distance (mm) | 90 |
| Rotation range per image () | 1 |
| Total rotation range () | 201 |
| Exposure time per image (s) | 180 |
| Space group | C2 |
| a, b, c () | 57.76, 39.53, 39.28 |
| , , () | 90, 108.33, 90 |
| Mosaicity () | 0.412 |
| Resolution range () | 301.36 (1.501.36) |
| Total No. of reflections | 96243 (15176) |
| No. of unique reflections | 17603 (4105) |
| Completeness (%) | 96.7 (89.5) |
| Average multiplicity | 5.5 (3.7) |
| I/(I) | 20.36 (3.63) |
| R merge † (%) | 8.2 (49.6) |
| R r.i.m. † (%) | 12.7 (49.9) |
| Overall B factor from Wilson plot (2) | 17.0 |
†
Diederichs Karplus (1997 ▶).