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. 2015 Jan 1;71(Pt 1):57–60. doi: 10.1107/S2053230X14025801

Table 3. Data collection and processing.

Values in parentheses are for the outer shell.

Beamline BL17U1, SSRF
Wavelength () 0.978918
Temperature (K) 100
Detector ADSC Q315r
Crystal-to-detector distance (mm) 400
Rotation range per image () 1
Total rotation range () 180
Exposure time per image (s) 1
Space group P212121
Unit-cell parameters (, ) a = 130.19, b = 139.36, c = 281.01, = = = 90.00
No. of molecules per asymmetric unit 8
Matthews coefficient (3Da1) 2.49
Solvent content (%) 50.54
Mosaicity () 0.388
Resolution range () 50.03.35 (3.473.35)
Total No. of reflections 548396
No. of unique reflections 74167
Completeness (%) 100 (100)
Multiplicity 7.4 (7.5)
I/(I) 17.2 (3.7)
R meas 0.144 (0.788)
R p.i.m. 0.053 (0.287)
Overall B factor from Wilson plot (2) 53.5