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. 2014 Dec 23;10:3111–3121. doi: 10.3762/bjoc.10.328

Table 1.

Gelation test results for amide derivatives I (6–14) and urea derivatives II (15–22).a

Compound Structure Hexane Water EtOH Water/DMSO (2:1) Water/EtOH (2:1)

6 graphic file with name Beilstein_J_Org_Chem-10-3111-i001.jpg I G 10.0 S G 7.4 G 8.0
7 graphic file with name Beilstein_J_Org_Chem-10-3111-i002.jpg I I G 10.0 G 4.0 G 4.0
8 graphic file with name Beilstein_J_Org_Chem-10-3111-i003.jpg C C G 20.0 G 5.4 G 6.0
9 graphic file with name Beilstein_J_Org_Chem-10-3111-i004.jpg I I G 20.0 G 5.7 G 5.7
10 graphic file with name Beilstein_J_Org_Chem-10-3111-i005.jpg I I G 10.0 G 4.6 G 8.0
11 graphic file with name Beilstein_J_Org_Chem-10-3111-i006.jpg C C G 20.0 G 5.0 G 8.8
12 graphic file with name Beilstein_J_Org_Chem-10-3111-i007.jpg C I S G 6.0 G 7.4
13 graphic file with name Beilstein_J_Org_Chem-10-3111-i008.jpg I G 2.0 G 8.0 G 5.7 G 10.0
14 graphic file with name Beilstein_J_Org_Chem-10-3111-i009.jpg C I G 10.0 G 20.0 G 10.0
15 graphic file with name Beilstein_J_Org_Chem-10-3111-i010.jpg I I G 10.0 G 4.0 G 2.0
16 graphic file with name Beilstein_J_Org_Chem-10-3111-i011.jpg I P G 5.0 G 2.0 G 2.0
17 graphic file with name Beilstein_J_Org_Chem-10-3111-i012.jpg P I G 5.0 G 4.0 G 3.3
18 graphic file with name Beilstein_J_Org_Chem-10-3111-i013.jpg C I G 10.0 G 5.0 G 5.0
19 graphic file with name Beilstein_J_Org_Chem-10-3111-i014.jpg I I G 2.5 G 2.0 G 1.3
20 graphic file with name Beilstein_J_Org_Chem-10-3111-i015.jpg P I G 3.3 G 4.0 G 4.0
21 graphic file with name Beilstein_J_Org_Chem-10-3111-i016.jpg I I G 6.6 G 2.8 G 5.0
22 graphic file with name Beilstein_J_Org_Chem-10-3111-i017.jpg I I G 20.0 G 4.0 G 5.0

aG, stable gel at room temperature, the number after G is the minimum gelation concentration (MGC) in mg/mL; I, insoluble; C, crystallization; P, precipitate; S, soluble at 20 mg/mL.