TABLE 2.
Data collection statistics of DHpERS1 Se-Met crystals
Statistics for the highest resolution shell are shown in parentheses.
| Se-Met peak | Se-Met inflection | |
|---|---|---|
| X-ray source | X12, DESY | X12, DESY |
| Wavelength (Å) | 0.9772 | 0.9777 |
| Resolution range (Å) | 47.3–3.0 (3.15–3.0) | 47.3–3.0 (3.15–3.0) |
| Temperature (K) | 100 | 100 |
| Crystal-to-detector distance (mm) | 272 | 272 |
| Rotation range per image (°) | 1.1 | 1.1 |
| Total rotation range (°) | 154 | 154 |
| Space group | C2221 | C2221 |
| Cell dimensions (Å) | a = 75.20, b = 99.09, c = 77.12 | a = 75.16, b = 99.07, c = 77.09 |
| Observed reflections | 36,987 (5,733) | 36,764 (5,768) |
| Unique reflections | 11,119 (1,743) | 11,090 (1,755) |
| Multiplicity | 3.3 (3.3) | 3.3 (3.3) |
| Rmerge (%) | 7.0 (26.0) | 7.3 (27.5) |
| Rpim (%) | 4.6 (17.1) | 4.8 (18.1) |
| Completeness (%) | 99.8 (99.1) | 99.9 (99.6) |
| I/σ(I) | 17.6 (6.1) | 16.8 (5.4) |