Table 1.
Crystallographic statistics.
Native | Se (peak) | |
---|---|---|
Crystal properties | ||
Space group | F4132 | F4132 |
Unit cell | ||
a, b, c (Å) | 292, 292, 292 | 294, 294, 294 |
α, β, γ (°) | 90, 90, 90 | 90, 90, 90 |
Data collection | ||
Wavelength (Å) | 1.11111 | 0.979663 |
Resolution range (Å) | 49.35-3.2 (3.28-3.2) | 169.5 - 3.7 (3.79-3.70) |
Total reflections | 239356 | 1006047 |
Unique reflections | 18127 | 21915 |
Completeness (%) | 100.00 (99.80) | 99.8 (99.3) |
Redundancy | 13.2 (13.6) | 45.9 (39.5) |
Rmeas (%) | 18.9 (194.4) | 20.4 (142.3) |
I/sigma (I) | 18.55 (1.70) | 26.96 (3.67) |
Wilson B-factor | 79.26 | 103.67 |
Refinement | ||
R-factor | 0.2280 | |
R-free | 0.2593 | |
Number of atoms | 3192 | |
Protein residues | 410 | |
RMS (bonds) | 0.013 | |
RMS (angles) | 1.59 | |
Ramachandran favored (%) | 97 | |
Ramachandran outliers (%) | 0.25 | |
Clashscore | 22.46 | |
Average B-factor | 89.5 |