Table 1.
Crystallographic statistics.
| Native | Se (peak) | |
|---|---|---|
| Crystal properties | ||
| Space group | F4132 | F4132 |
| Unit cell | ||
| a, b, c (Å) | 292, 292, 292 | 294, 294, 294 |
| α, β, γ (°) | 90, 90, 90 | 90, 90, 90 |
| Data collection | ||
| Wavelength (Å) | 1.11111 | 0.979663 |
| Resolution range (Å) | 49.35-3.2 (3.28-3.2) | 169.5 - 3.7 (3.79-3.70) |
| Total reflections | 239356 | 1006047 |
| Unique reflections | 18127 | 21915 |
| Completeness (%) | 100.00 (99.80) | 99.8 (99.3) |
| Redundancy | 13.2 (13.6) | 45.9 (39.5) |
| Rmeas (%) | 18.9 (194.4) | 20.4 (142.3) |
| I/sigma (I) | 18.55 (1.70) | 26.96 (3.67) |
| Wilson B-factor | 79.26 | 103.67 |
| Refinement | ||
| R-factor | 0.2280 | |
| R-free | 0.2593 | |
| Number of atoms | 3192 | |
| Protein residues | 410 | |
| RMS (bonds) | 0.013 | |
| RMS (angles) | 1.59 | |
| Ramachandran favored (%) | 97 | |
| Ramachandran outliers (%) | 0.25 | |
| Clashscore | 22.46 | |
| Average B-factor | 89.5 | |