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. 2015 Jan 1;71(Pt 1):28–30. doi: 10.1107/S2056989014026309

Table 2. Experimental details.

Crystal data
Chemical formula C19H16N2O
M r 288.34
Crystal system, space group Monoclinic, P21
Temperature (K) 100
a, b, c () 7.704(6), 16.706(12), 11.617(9)
() 93.880(14)
V (3) 1492(2)
Z 4
Radiation type Mo K
(mm1) 0.08
Crystal size (mm) 0.20 0.15 0.12
 
Data collection
Diffractometer Bruker SMART APEX CCD
Absorption correction Multi-scan (SADABS; Sheldrick, 2004)
T min, T max 0.986, 0.990
No. of measured, independent and observed [I > 2(I)] reflections 8013, 5245, 4091
R int 0.026
(sin /)max (1) 0.606
 
Refinement
R[F 2 > 2(F 2)], wR(F 2), S 0.045, 0.127, 0.97
No. of reflections 5242
No. of parameters 397
No. of restraints 1
H-atom treatment H-atom parameters constrained
max, min (e 3) 0.12, 0.15

Computer programs: SMART and SAINT (Bruker, 2003), SIR97 (Altomare et al., 1999), SHELXL97 (Sheldrick, 2008), DIAMOND (Brandenberg Putz, 2006), Mercury (Macrae et al., 2008) and PLATON (Spek, 2009).