| Crystal data |
| Chemical formula |
C36H44O10C6H6
|
|
M
r
|
714.82 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
90 |
|
a, b, c () |
9.6397(6), 13.6008(8), 15.0461(10) |
| , , () |
83.6966(19), 77.488(2), 77.9768(18) |
|
V (3) |
1879.2(2) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.09 |
| Crystal size (mm) |
0.50 0.37 0.19 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Venture |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2013 ▸) |
|
T
min, T
max
|
0.96, 0.98 |
| No. of measured, independent and observed [I > 2(I)] reflections |
25389, 6526, 5180 |
|
R
int
|
0.043 |
| (sin /)max (1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.042, 0.151, 0.93 |
| No. of reflections |
6526 |
| No. of parameters |
475 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.25, 0.25 |
